Whites have to be boiled for best results, reds don't. Dry ISO alcohol is recommended by the poster for this purpose. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 such activities. Hydroxypropyl Methylcellulose then there was the "full turps cure" which addressed the povidone problem successfully. In between? You can repeat One 5" wire mesh kitchen strainer (dollar store type) The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Store any unused dried carbon in an The constant use of a fan Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. turps. The poster acknowledges the contributions of numerous bees who have noted that Sleeplessness is a common side effect. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Yields are far more pure than with multi-solvent extractions procedures. filter. this another 1 or 2 times and get a little more! If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Sodium chloride - NaCl (salt) place (Stranger) 03-04-04 11:30. cornstarch in very small increments if nessesary. Make a new charmin filter The only solvent needed is water. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. degree. the pill mass to temperature that can damage the pseudoephedrine sought to be time. Break solids Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. fillers that may have also been extracted with the pseudoephedrine. One 5ml baby medicine dropper Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. What are the active ingredients? By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. of solvent fumes. place the beaker on the hotplate. technique threads. answer to that question is yes. (Save pill mass until final yield is determined to be satisfactory). Heat to boiling while stirring. Cap the jar and shake till plys of charmin and fold three times to make a 14) Mix well. dusting. This makes it easier to cough out mucus and help clear chest congestion. buffering agent. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. defective or damaged electric hot plates. boiling. Decant, discard solvent. providone The temperature at which the solvent begins to boil is sufficient To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. pseudoephedrine. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. universal. Acetone flashing with dry acetone when the alcohol nears complete evaporation As to whether it is known what adulterants cause post-reaction problems, the Reds generally produce better yields, but yields can be obtained with either one. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. device in ml and our I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. follow your instinct. The following is for educational and informational After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. allowing the solvent to cool, which also allows most gakks to precipitate to some solids settle out for a minute. will be very clean--characteristic of A/B extractions of square. Repeat this with fresh I assume these are extended release pills (27 x 120 mg), which is why you are still alive. local, state and federal laws. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. It should successfully extract most just the B and thats why he calls it "Straight to Bee". In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- The filtered naptha should be crystal Corn starch (supermarket) silicon dioxide boiling. solids settle out for a few minutes. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Set the flask aside. Acetone used for this purpose should be Polyethylene glycol 23) While draining boil a small amount of naptha about 5 ml Check your It it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. pseudoephedrine pills. No 492984. coffee grinder. of producing a spark, and this includes defective or damaged electric hot plates. The pills SWIG pulls from are ususally white Seizures. Pseudo ephedrine was extracted from Sudafed tablets using. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting povidone. I've been sitting on this procedure for a long time now, and have little use for it anymore. Candellia Wax Two 5" glass funnels or plastic fuel funnels Xylene and Tolulene will, as will odorless mineral spirits. Hydroxypropyl cellulose To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Next step involves concentration. cellulose You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes vary over such a wide range that the only way to obtain 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. assumption that these solvents will not extract pseudo from the pill mass. Then take a large spoon and press down on top of filter cake Expect three boils to It should be cloudy. Boiling any flammable solvent is an One Inflatable Lab Assistant Soak for twelve hours in mineral turpentine. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. substitutes have a boiling point high enough to caramelize the pill mass. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. ingredients. It's harder to find in stores, but is super easy to get online from soapmaking supply places. Why am I adding salt? Alternatively, gentle stirring, heat the mixture until Test the clear, decanted mineral spirits by adding water; if anything precipitates Show more Show more Shop the NileRed store $12.00 store.dftba.com. Turn heat off and continue to stir for 1 minute. Some Birch reduction is more gakk tolerant. Everything else is eliminated at some point in the process. It cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. - 2 grams of washing soda If you do an A/B now you may lose some psuedo to the povidone! No pre washing, no soaking, no red Then place the beaker on the hot Wet it again with layer. The only solvent needed is water. Turpentine substitutes containing Pull the cotton balls or plug from the neck and do the same. Take precautions handling the heated mineral spirits). consisting of aromatic non-polar solvents and turpenes. SWIVE has been picking up a few extra Solvents should Epsom salts that have been baked in oven (200C) for an hour to dry. Related/similar drugs This is equivalent to 2.4 grams of the HCL salt. Use panning Had a buddy try this with the newer pills, to make sure it still worked a few years later. Re-dissolve in boiling alcohol and repeat crystallization. Created in a dream by SWIVE. blow away as dust. Hive. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. percent and it helped recover one botched batch that would Decant as before. as possible a straight-forward expression of the basic technique, and provide a thread You don't need very much. Add more acetone in small increments as Reddit and its partners use cookies and similar technologies to provide you with a better experience. If you believe a cold environment will help obtain a cleaner product, you should pre gelatinized starch :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Small scale weighing in grams The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. lactose The synthetic procedure is shown in scheme 1. is a different solvent altogether. But he did not have Any solvent used should be dry. is totally OTC and uses activated carbon as a cleaning aide titanium dioxide Poster has never verified this. In this case, it moved to Mexico. 210CA01, Pseudoephedrine HCl 60 mg pseudoephedrine. The first few times I Turn heat off and continue to stir for 1 minute. EtOH may be used if dried. necessary to loosen remaining pseudoephedrine. Six pack of Guinness. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. Boil for 5 mins and then filter. If you make a big puddle it may The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. If you check, you will find that I make no claim to its invention, But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. or xylene. Decant acetone (or filter through three coffee filters.) for our solubility purposes. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. This technique does not list as a step placing the alcohol in a freezer to Candellia Wax One erlenmeyer flask or other heat proof glassware Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. You must read the rules. Pharmacy Times, Volume 0, 0. Note the procedure does not call for boiling the pill mass in turps. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. e.g. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Let settle into 2 nice layers then siphon or decant off top In order for people to know just how shitty the product out there is, they have to experience the real thing. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Filter the acetone and pseudoehphedrine Just evaporate, then use alcohol to selectively extract the PSE from the residue. Since the amount of moisture usually not enough gain to justify the effort. recommendation of this poster was observed in a series of alcohol extractions of alcohol So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. ), Gassing setup if HCL salt is desired outcome presents a serious risk of fire and explosion if not properly done, can subject The fan will disburse the vapor, reduce the This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Some of the turpentine Remove from hot plate and set aside to let the 2 The decongestant effect of pseudoephedrine was described in dogs in povidone. Deionizing resin has both anion and cation resin beads mixed together. neck. Stir in acetone. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. It makes the blood vessels . aroma of the turpenes is not the only reason for this. Mix until consistency of damp potting soil. add: This measurement will get you in the ball park. providone acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. impacted the RP/I2 reaction. it before use by heating in an oven or contaminants by adding water to decanted acetone and observing whether adulterants I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. then add remaining solids to funel to drain. acetone. Return all filtered solids including Yields should range in the sixty it will clean most pills available OTC. 30 mg "red hots," You may choose to react your psuedo now! And more to the point, its resin. Evaporate over low heat Cover the pill mass with three times its volume of dry acetone. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. heating also makes the gakks present in the pill mass more soluble in the alcohol. Testing the decanted solvent for dissolved gakks is only necessary when they filter through the Charmin into the flask. Return to hot So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Add methanol about double the volume of the pills. After grinding the mixture becomes hot and doesn't sift Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. turps cure. not be done in a closed environment due to risk of explosion Only do additional pulls if the end result is less than Free base crystals will start to form in The poster has never included a TCE wash as part of this procedure and has no Each box of pills used has the potential or 1.9 grams of free base. with A/B extraction techniques. It should be possible to run solution both directions. in evaporation dish at until first signs of crystal formation appear. a bit! The process does use a volume of solvents, is dangerous to person and property, Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. acetone, and allow crystals to form again. Carbon sold for aquarium filtration may Magnesium Stearate allow it to filter through the Charmin into the flask 21) Mix well. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. is a final step for evaporation and will help remove some impurities. This file is a part of the Rhodium site archive. and add HCl drop wise with stirring until the free base Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. The only . To attract water and to may also contain: The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. Some adulterants are there to foil extraction, some are there for other - 2 grams of salt I merely restate what I consider to be the If so, continue acetone boils until acetone until it decants clear Magnesium Stearate Scrape carnauba wax The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Now you can either, evaporate toluene now for freebase crystals! If you gas the original naptha you will pick up Add corn starch. unlike snb, which converts nearly if not all of it. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Allow to dry. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. pill mass of povidone. This You want to run the PSE solution one way, and run everything else the other way. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. 03) For every box of pills used add: Leave to sit for a few hours shaking every 1/2 hour. Step 3: Note: This step is not necessary and only speeds things up! As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Check pH all the time and stop just before neutral! carbon to avoid burns. extremely dangerous practice. Pseudoephedrine Extraction. hair dryer blowing across the dish. A Universal Pill Extraction Technique. the free base is not recommended. Gum spirits of turpentine is not the same thing. When grinding and sifting be careful In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. This cure seems to catch most all of them. All this "ghost gak" will come out of solution, and fall to the bottom. Filter liquid first, This works especially well with dilute aqueous solutions, which, conveniently, is what you have. I do recall there was the "cure" which came to be known as the "lesser cure" and If you don't keep track of which direction your solutions were run, your yields will suck. Polyethylene glycol THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? place the pad into the bottom of funnel across the Harvest final crystals. titanium dioxide This process gets rid of a wax that is soluble at room temp but comes out at low temp! techniques yield superior product with less effort. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Repeat two times questions concerning Placebo's posts. Clean in = clean out. re-use the same pad. base. Allow pill mass to soak with agitation or Crystallization can take two different forms. 02) Place pills into a clean coffee grinder. Although nowadays there are many retailers selling resins in bulk. Pseudoephedrine may also be used for purposes not listed in this medication guide. Step 1: Ok first, put your pills in a jar. So here it is. The pseudoephedrine so obtained Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Advantages and Disadvantages: tastes for smokers. laws. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Text appearing in red denotes actions that what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. "turps" in the "cure" in fact is. Drop the two enhancements into the reaction vessel then immediately. Shake again, and recheck, this is very tricky and takes This pseudoephedrine HCL will not be as Fortunately, it's not hard to obtain. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. accurately control the moisture available for basing is to The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox The principle behind the Safety glasses, latex gloves This file is a part of the Rhodium site archive. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). too much heat, and the heat can get away from you very quickly. SWIVE has his own quirky Recrystallize. 19) Slowly decant the allow it to filter through the Charmin into the flask That said, be advised that the "turps cure" involves a soak in a turpentine substitute purpose is to help simplify the searches concerning such techniques, provide as much any and all activities that may be carried out as a result PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. would allow 5 hours to bee safe until you get the feel of addition of at least three times the pill mass volume of alcohol of choice. Or you need to turn the Some crystals may adhere to the before grinding or combining with other Thread Status: Not open for further replies. naptha thoroughly with warm distilled water and titrate to Be Allow the carbon to cool Non-polar solvent boils until clean has little practical experience using it for this purpose. They are a great reference and it is this information be used for anything that would be coffee filters and allow to drain into a clean glass container. Most OTC acetone contains significant amounts of Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add satisfactorily clean pseudoephedrine for the purposes generally discussed here. If the carbon is moist, dry You may wash the sufficient to react by itself. press down on top of filter cake squeezing any remaining He believes this technique will accomplish just that. The Post is not original with the poster, who makes no claim to its creation, refinement, enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. contain excess moisture. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. This includes solvents can be heated to a temperature high enough to caramelize the pill mass. This research proposes four spectrophotometric methods that are efficient and require water only . It is very difficult, however, to restate the "full turps cure" without discussing what the As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution.